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" Macroscale and microscale organic experiments "
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BL
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| Record Number
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705566
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| Doc. No
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b527755
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| Main Entry
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Williamson, Kenneth L
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| Title & Author
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Macroscale and microscale organic experiments
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| Edition Statement
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6th ed. // Kenneth 1. Williamson, Katherine M. Masters
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| Publication Statement
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Belmont, CA :: Brooks/Cole,, ©2011
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| Page. NO
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xiii, 802 pages :: illustrations ;; 29 cm
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| ISBN
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0538733330
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: 9780538733335
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| Notes
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Includes index
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| Contents
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1. Introduction. -- 2. Laboratory Safety, Courtesy, and Waste Disposal Techniques. -- 3. Melting Points and Boiling Points. -- 4. Recrystallization. -- 5. Distillation. -- 6. Steam Distillation, Vacuum Distillation, and Sublimation. -- 7. Extraction. -- 8. Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste. -- 9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments. -- 10. Gas Chromatography: Analysis of Alkene Isomers. -- 11. Infrared Spectroscopy. -- 12. Nuclear Magnetic Resonance Spectroscopy. -- 13. Mass Spectroscopy. -- 14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis. -- 15. Computational Chemistry Elimination, Substitution, and Addition. -- 16. The SN2 Reaction: 1-Bromobutane. -- 17. Nucleophilic Substitution Reactions of Alkyl Halides. -- 18. Radical Initiated Chlorination of 1-Chlorobutane. -- 19. Alkenes from Alcohols: Cyclohexene from Cyclohexanol. -- 20. Bromination and Debromination: Purification of Cholesterol. -- 21. Dichlorocarbene Oxidation and Reduction. -- 22. Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid. -- 23. The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent. -- 24. Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol. -- 25. Catalytic Hydrogenation. -- 26. Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis. -- 27. Epoxidation of Cholesterol. Aromatic Substitution and Elimination. -- 28. Nitration of Methyl Benzoate -- 29. Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry. -- 30. Alkylation of Mesitylene. -- 31. The Friedel-Crafts Reaction: Anthraquinone and Anthracene. -- 32. Friedel-Crafts Acylation of Ferrocene: Acetylferrocene. -- 33. Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical. -- 34. 1,2,3,4-Tetraphenylnaphthalene via Benzyne. -- 35. Triptycene via Benzyne Reactions of Aldehydes and Ketones. -- 36. Aldehydes and Ketones. -- 37. Dibenzalacetone by the Aldol Condensation. -- 38. Grignard Synthesis of Triphenylmethanol and Benzoic Acid. -- 39. The Wittig and Wittig-Horner Reactions Reactions of Carboxylic Acids, Esters, and Amines. -- 40. Esterification and Hydrolysis. -- 41. Acetylsalicylic Acid (Aspirin). -- 42. Malonic Ester of a Barbiturate. -- 43. Amines. -- 44. The Sandmeyer Reaction: 1-Bromo-4-chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene. -- 45. Synthesis and Bioessay of Sulfanilamide and Derivatives. -- 46. Dyes and Dyeing. -- 47. Martius Yellow. -- 48. Diels-Alder Reaction. -- 49. Ferrocene [Bis(cyclopentadienyl)iron]. -- 50. A Diels-Alder Reaction Puzzle: The Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride. -- 51. Tetraphenylcyclopentadienone. -- 52. Hexaphenylbenzene and Dimethyl Tetraphenylphthalate. Derivatives of 1,2-Diphenylethane: A Multistep Synthesis. -- 53. The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine. -- 54. Nitric Acid Oxidation; Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline. -- 55. Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil. -- 56. The Synthesis of 2,2-Dimethyl-1,5-dioxolane; The Acetonide Derivative of a Vicinal Diol. -- 57. The 1,4-Addition: Reductive Acetylation of Benzil. -- 58. Synthesis of an Alkyne from an Alkene; Bromination and Dehydrobromination: Stilbene and Diphenylacetylene. -- 59. The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid. -- 60. Multicomponent Reactions: The Aqueous Passerini Reaction. -- 61. Chemiluminescence: Syntheses of Cyalume and Luminol. -- 62. Photochemistry: The Synthesis of Benzopinacol Natural Product Chemistry and Biochemistry. -- 63. Carbohydrates and Sweeteners. -- 64. Virstatin, a Possible Treatment for Cholera. -- 65. Biosynthesis of Ethanol and Enzymatic Reactions. -- 66. The Synthesis of Natural Products: Pseudopellitierene and Camphor. -- 67. Polymers: Synthesis and Recycling. -- 68. Searching the Chemical Literature
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| Subject
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Chemistry, Organic, Laboratory manuals
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| Dewey Classification
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547.0078
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| LC Classification
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QD261.W54 2011
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| Added Entry
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Masters, Katherine M
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